Repealed by Commission Regulation (EU) No 10/2011 of 14 January 2011 on plastic materials and articles intended to come into contact with food Text with EEA relevance.

http://www.legislation.gov.uk/eudr/1980/766Commission Directive of 8 July 1980 laying down the Community method of analysis for the official control of the vinyl chloride monomer level in materials and articles which are intended to come into contact with foodstuffs (80/766/EEC) (repealed)Commission Directive of 8 July 1980 laying down the Community method of analysis for the official control of the vinyl chloride monomer level in materials and articles which are intended to come into contact with foodstuffs (80/766/EEC) (repealed)2020-12-12King's Printer of Acts of Parliamenttexttext/xmlenhttp://www.nationalarchives.gov.uk/webarchive/2011-04-30

Commission Directive

of 8 July 1980

laying down the Community method of analysis for the official control of the vinyl chloride monomer level in materials and articles which are intended to come into contact with foodstuffs

(80/766/EEC) (repealed)

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Article 1

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Article 2

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Article 3

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ANNEXDETERMINATION OF THE VINYL CHLORIDE MONOMER LEVEL IN MATERIALS AND ARTICLES1.SCOPE AND FIELD OF APPLICATION

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2.PRINCIPLE

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3.REAGENTS3.1.

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3.2.

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3.3.

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4.APPARATUS4.1.

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4.2.

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4.3.Gas-chromatographic column.

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4.4.Sample phials or flasks fitted with silicon or butyl rubber septa.

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4.5.

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4.6.

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4.7.

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5.PROCEDURE

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5.1.Preparation of concentrated standard VC solution at approximately 2 000 mg/kg

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5.2.Preparation of dilute standard VC solution

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5.3.Preparation of the calibration curve

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5.4.Validation of preparation of standard solutions obtained in points 5.1 and 5.2

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5.5.Preparation of the samples of materials or articles

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5.6.Gas-chromatographic determinations5.6.1.

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5.6.2.

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5.6.3.

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5.6.4.

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6.CALCULATION OF THE RESULTS6.1.Find by interpolation on the curve, the unknown concentration of each of the two solutions of the sample taking account of the internal standard solution if used. Calculate the amount of VC in each of the two samples of material or article under investigation by applying the following formula:

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6.2.

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7.CONFIRMATION OF THE VC LEVEL

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8.REPEATABILITY

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Repealed by
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<p>laying down the Community method of analysis for the official control of the vinyl chloride monomer level in materials and articles which are intended to come into contact with foodstuffs</p>
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. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
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. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
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ANNEX
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<heading>DETERMINATION OF THE VINYL CHLORIDE MONOMER LEVEL IN MATERIALS AND ARTICLES</heading>
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1.
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<level eId="annex-division-3-division-3.2" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
3.2.
</num>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
<level eId="annex-division-3-division-3.3" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
3.3.
</num>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
</level>
<level eId="annex-division-4" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
4.
</num>
<heading>APPARATUS</heading>
<level eId="annex-division-4-division-4.1" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
4.1.
</num>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
<level eId="annex-division-4-division-4.2" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
4.2.
</num>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
<level eId="annex-division-4-division-4.3" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
4.3.
</num>
<heading>Gas-chromatographic column.</heading>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
<level eId="annex-division-4-division-4.4" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
4.4.
</num>
<heading>Sample phials or flasks fitted with silicon or butyl rubber septa.</heading>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
<level eId="annex-division-4-division-4.5" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
4.5.
</num>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
<level eId="annex-division-4-division-4.6" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
4.6.
</num>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
<level eId="annex-division-4-division-4.7" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
4.7.
</num>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
</level>
<level eId="annex-division-5" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
5.
</num>
<heading>PROCEDURE</heading>
<intro>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</intro>
<level eId="annex-division-5-division-5.1" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
5.1.
</num>
<heading>
<strong>Preparation of concentrated standard VC solution at approximately 2 000 mg/kg</strong>
</heading>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
<level eId="annex-division-5-division-5.2" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
5.2.
</num>
<heading>
<strong>Preparation of dilute standard VC solution</strong>
</heading>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
<level eId="annex-division-5-division-5.3" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
5.3.
</num>
<heading>
<strong>Preparation of the calibration curve</strong>
</heading>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
<level eId="annex-division-5-division-5.4" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
5.4.
</num>
<heading>
<strong>Validation of preparation of standard solutions obtained in points 5.1 and 5.2</strong>
</heading>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
<level eId="annex-division-5-division-5.5" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
5.5.
</num>
<heading>
<strong>Preparation of the samples of materials or articles</strong>
</heading>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
<level eId="annex-division-5-division-5.6" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
5.6.
</num>
<heading>
<strong>Gas-chromatographic determinations</strong>
</heading>
<level eId="annex-division-5-division-5.6-division-5.6.1" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
5.6.1.
</num>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
<level eId="annex-division-5-division-5.6-division-5.6.2" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
5.6.2.
</num>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
<level eId="annex-division-5-division-5.6-division-5.6.3" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
5.6.3.
</num>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
<level eId="annex-division-5-division-5.6-division-5.6.4" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
5.6.4.
</num>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
</level>
</level>
<level eId="annex-division-6" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
6.
</num>
<heading>CALCULATION OF THE RESULTS</heading>
<level eId="annex-division-6-division-6.1" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
6.1.
</num>
<heading>Find by interpolation on the curve, the unknown concentration of each of the two solutions of the sample taking account of the internal standard solution if used. Calculate the amount of VC in each of the two samples of material or article under investigation by applying the following formula:</heading>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
<level eId="annex-division-6-division-6.2" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
6.2.
</num>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
</level>
<level eId="annex-division-7" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
7.
</num>
<heading>CONFIRMATION OF THE VC LEVEL</heading>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
<level eId="annex-division-8" period="#period1" class=" repealed">
<num>
<noteRef href="#c000001" marker="F1" class="commentary F"/>
8.
</num>
<heading>REPEATABILITY</heading>
<content>
<p>. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .</p>
</content>
</level>
</hcontainer>
</hcontainer>
</body>
</act>
</akomaNtoso>