ANNEX IU.K.

E 214 ETHYL p-HYDROXYBENZOATEU.K.

SynonymsEthylparaben
Ethyl p-oxybenzoate
Definition
Chemical nameEthyl-p-hydroxybenzoate
Ethyl ester of p-hydroxybenzoic acid
Einecs204-399-4
Chemical formulaC9H10O3
Molecular weight166,8
AssayContent not less than 99,5 % after drying for two hours at 80 oC
DescriptionAlmost odourless, small, colourless crystals or a white, crystalline powder
Identification
A.Melting range
115 oC to 118 oC
B.Positive test for p-hydroxybenzoate
Melting range of p-hydroxybenzoic acid isolated by acidification and not recrystallised: 213 oC to 217 oC, after vacuum drying in a sulphuric acid desiccator
C.Positive test for alcohol
Purity
Loss on dryingNot more than 0,5 % after drying for two hours at 80 oC
Sulphated ashNot more than 0,05 %
p-Hydroxybenzoic acid and salicylic acidNot more than 0,35 % expressed as p-hydroxybenzoic acid
ArsenicNot more than 3 mg/kg
LeadNot more than 5 mg/kg
MercuryNot more than 1 mg/kg
Heavy metals (as Pb)Not more than 10 mg/kg