[F1 ANNEX XVII U.K. METHOD FOR THE DETERMINATION OF STIGMASTADIENES IN VEGETABLE OILS

Textual Amendments

F1 Inserted by Commission Regulation (EC) No 656/95 of 28 March 1995 amending Regulation (EEC) No 2568/91 on the characteristics of olive oil and olive-residue oil and on the relevant methods of analysis and Council Regulation (EEC) No 2658/87 on the tariff and statistical nomenclature and on the Common Customs Tariff.

Figure 1 U.K.

Gas chromatograms obtained from olive oil samples analysed on a fused silica capillary column (0,25 mm internal diameter by 25 m) coated with 5 %-phenylmethylsilicone, 0,25 μm film thickness. U.K.

(a)

First fraction (30 ml) from a virgin oil, spiked with standard.

(b)

Second fraction (40 ml) from an olive oil containing 0,10 mg/kg of stigmastadienes.

(c)

Second fraction (40 ml) containing a small proportion of the first fraction.]