Please note that the date you requested in the address for this web page is not an actual date upon which a change occurred to this item of legislation. You are being shown the legislation from , which is the first date before then upon which a change was made.

ANNEXU.K.

a

Details of the analytical methods are available at the following address of the Reference Laboratory: http://irmm.jrc.ec.europa.eu/EURLs/EURL_feed_additives/Pages/index.aspx

b

Easy to ensile forage: > 3 % soluble carbohydrates in fresh material (e.g. whole plant maize, ryegrass, brome grass or sugar beet pulp). Commission Regulation (EC) No 429/2008 (OJ L 133, 22.5.2008, p. 1).

c

As propionic acid.

Identification number of the additiveName of the holder of authorisationAdditiveComposition, chemical formula, description, analytical methodSpecies or category of animalMaximum ageMinimum contentMaximum contentOther provisionsEnd of period of authorisation
mg/kg of complete feedingstuff with a moisture content of 12 %
Category of technological additives. Functional group: silage additives
1k280Propionic acid
  • Additive composition

    Propionic acid ≥ 99,5 %

  • Characterisation of the active substance

    • Propionic acid ≥ 99,5 %

    • C3H6O2 CAS No: 79-09-4

    • Non-volatile residue ≤ 0,01 % when dried at 140 °C to constant weight

    • Aldehydes ≤ 0,1 % expressed as formaldehyde

    • Produced by chemical synthesis

  • Method of Analysis a

    Quantification of propionic acid as total propionic acid in feed additive, premixtures, feedingstuffs: ion exclusion High Performance Liquid Chromatography with refractive index (HPLC-RI)

Ruminants

1.The simultaneous use of other organic acids at the maximum permitted doses is contraindicated.

20 December 2023
Pigs30 000
Poultry10 000
1k281Sodium propionate
  • Additive composition

    Sodium propionate ≥ 98,5 %

  • Characterisation of the active substance

    • Sodium propronate ≥ 98,5 %

    • C3H5O2Na

    • CAS No: 137-40-6

    • Loss on drying ≤ 4 % determined by drying for two hours at 105 °C

    • Water insolubles ≤ 0,1 %

    • Produced by chemical synthesis

  • Method of Analysis a

    Quantification of sodium propionate in feed additive:

    (1)

    ion exclusion High Performance Liquid Chromatography with refractive index detection (HPLC-RI) – for the determination of total propionate; and

    (2)

    atomic absorption spectrometry, AAS (EN ISO 6869) – for the determination of total sodium.

    Quantification of sodium propionate as total propionic acid in premixtures, feedingstuffs: ion exclusion High Performance Liquid Chromatography with refractive index (HPLC-RI)

Ruminants

1.The simultaneous use of other organic acids at the maximum permitted doses is contraindicated.

20 December 2023
Pigs30 000c
Poultry10 000c
1k284Ammonium propionate
  • Additive composition

    Preparation of ammonium propionate ≥ 19,0 %, propionic acid ≤ 80,0 % and water ≤ 30 %

  • Characterisation of the active substance

    • Ammonium propionate: C3H9O2N

    • CAS No: 17496-08-1

    • Produced by chemical synthesis

  • Method of Analysis a

    Quantification of the ammonium propionate in feed additive:

    (1)

    ion exclusion High Performance Liquid Chromatography with refractive index detection (HPLC-RI) – for the determination of total propionate; and

    (2)

    titration with sulphuric acid and sodium hydroxide for the determination of ammonia.

    Quantification of ammonium propionate as total propionic acid in premixtures, feedingstuffs:

    ion exclusion High Performance Liquid Chromatography with refractive index (HPLC-RI)

Ruminants

1.The simultaneous use of other organic acids at the maximum permitted doses is contraindicated.

20 December 2023
Pigs30 000c
Poultry10 000c