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Commission Regulation (EU) 2017/2158 of 20 November 2017 establishing mitigation measures and benchmark levels for the reduction of the presence of acrylamide in food (Text with EEA relevance)
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Wherever possible the trueness of analysis shall be estimated by including suitable certified reference materials in the analysis.
Parameter | Criterion |
---|---|
Applicability | Foods specified in this Regulation |
Specificity | Free from matrix or spectral interferences |
Field blanks | Less than Limit of Detection (LOD) |
Repeatability (RSDr) | 0,66 times RSDR as derived from (modified) Horwitz equation |
Reproducibility (RSDR) | as derived from (modified) Horwitz equation |
Recovery | 75-110 % |
Limit of Detection (LOD) | Three tenths of LOQ |
Limit of Quantification (LOQ) | For benchmark level < 125 μg/kg: ≤ two fifths of the benchmark level (however not required to be lower than 20 μg/kg) For benchmark level ≥ 125 μg/kg: ≤ 50 μg/kg |
If the analytical result, corrected for recovery but not taking into account the measurement uncertainty, indicates that a product has exceeded the benchmark level, or contains acrylamide at a level higher than anticipated (taking into account previous analyses, but lower than the benchmark level), then the FBOs shall carry out a review of the mitigation measures applied and shall take additional available mitigation measures to ensure that acrylamide level in the finished product is below the benchmark level. This must be demonstrated by the undertaking of a new representative sampling and analysis, after the introduction of the additional mitigation measures.
FBOs shall make the analytical results obtained from the analysis every year available on request to the competent authority together with descriptions of the products analysed. Details of mitigation measures taken to reduce levels of acrylamide below the benchmark level shall be provided for those products exceeding the benchmark level.
M. Thompson et al, Pure and Applied Chemistry, 2006, 78, pp. 145-196.
Edited by M. Thompson and R. Wood, Pure and Applied Chemistry, 1995, 67, pp. 649-666.
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