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7.5 Set up the spectrophotometer (5.1), at a wavelength of 285.2 nm using an oxidising air-acetylene flame. Spray successively, in triplicate, the standard solutions (7.4), the sample solution (7.2) and the blank solution (7.3), washing the instrument through with distilled water between each spraying. Plot the calibration curve using the mean absorbances as the ordinates and the corresponding concentrations of magnesium in μg/ml as the abscissae. Determine the concentration of magnesium in the sample and blank by reference to the calibration curve.
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