SCHEDULE 2METHODS OF ANALYSIS

13b.DETERMINATION OF TOTAL MAGNESIUM —EDTA METHOD

4.2    REAGENTS

EDTA solution 0.05 M: dissolve 18.61 g of the dihydrated disodium salt of ethylenediaminetetra-acetic acid in 600-800 ml water contained in a 1 litre beaker. Transfer the solution quantitatively into a 1 litre graduated flask, make up to volume with water and mix. Check this solution with solution (4.1) by taking a sample of 20 ml of the latter and titrating following analytical procedure 7.3.1.

1 ml of the EDTA solution should correspond to 1.216 mg of Mg or 2.016 mg of MgO and to 2.004 mg of Ca or 7.804 mg of CaO.