The Fertilisers (Sampling and Analysis) Regulations 1991

16. DETERMINATION OF FINENESS OF PRODUCTS OTHER THAN POTASSIC BASIC SLAG

SCOPE AND FIELD OF APPLICATION

1.  This method is applicable to “Rock phosphate” in Group 2(b) and to products in Groups 4(c), 5(a) and 5(b) of Section A of the Table in Schedule I of the Fertilisers Regulations 1990(1).

PRINCIPLE

2.  By hand sieve shaking, the proportion of material passing through the prescribed sieve is determined.

APPARATUS

3.  Sieves having square apertures of 45 mm, 6.7 mm, 6.3 mm, 5 mm, 3.35 mm, 1.0 mm and 150 microns; lower receiver to fit sieve. Test sieves conforming to British Standard 410: 1986 are suitable.

PROCEDURE

For sieving through 3.5 mm, 1.0 mm and 150 micron sieves

4.—4.1 Thoroughly mix the sample and quarter down until a portion of about 100 g is obtained. Heat this portion at 1OO°C until dry and thoroughly mix. Weigh to the nearest 0.01 g, 20 g and transfer to the sieve with the lower receiver attached. Proceed as described in 4.4.

For sieving through 6.7 mm, 6.3 mm and 5 mm sieves

4.2 Oven dry the sample at 1OO°C for 24 hours and thoroughly mix. Weigh to the nearest 0.1 g, 200 g and transfer to the sieve with the lower receiver attached. Proceed as described in 4.4.

For sieving through a 45 mm sieve

4.3 If the sample appears moist or damp, oven dry at 1OO°C for 24 hours, but if the sample appears dry, heating is not necessary. Thoroughly mix the sample and weigh to the nearest 0.1 g, 500 g and transfer to the sieve with the lower receiver attached. Proceed as in 4.4.

Sieving

4.4 Shake the sieve for 5 minutes, frequently tapping the side. Disintegrate soft lumps such as can be caused to crumble by the application of the fibres of a soft brush, taking care that the hard part of the brush does not make contact with the sieve and that the brush is not used to brush particles through the sieve. Brush out the powder in the lower receiver and weigh. Replace the receiver and repeat the shaking and tapping procedure for 2 minutes. Add the powder in the receiver to the first portion and weigh. Repeat the process until not more than 0.04 g passes through the seive during 2 minutes.

EXPRESSION OF RESULTS

5.  Calculate the fineness by expressing the weight of the material passing through the sieve as a percentage of the weight of the portion of the dried (or as the case may be, undried) sample taken for sieving.

(1)

S.I. 1990/887.